MassachusettsDepartmentofEnvironmentalProtectionBureauofWasteSiteCleanupWSC-CAMSection:VAJuly1,2010RevisionNo.1FinalPageofNUMPAGES32QualityControlRequirementsandPerformanceStandardsfortheAnalysisofPolychlorinatedBiphenyls(PCBs)byGasChromatography(GC)inSupportofResponseActionsundertheMassachusettsContingencyPlan(MCP)MassachusettsDepartmentofEnvironmentalProtectionBureauofWasteSiteCleanupQualityAssuranceandQualityControlRequirementsandPerformanceStandardsforSW-846Method8260B,VolatileOrganicCompoundsbyGasChromatography/MassSpectrometry(GC/MS)BWSC-CAMSection:IIA8February2002RevisionNo.1InterimFinalPageofNUMPAGES32Title:TableIIA-1SpecificQA/QCRequirementsandPerformanceStandardsforSW-846Method8260B(Page1of3ofTableIIA-1)WSC–CAM–VAQualityControlRequirementsandPerformanceStandardsfortheAnalysisofPolychlorinatedBiphenyls(PCBs)byGasChromatography(GC)inSupportofResponseActionsundertheMassachusettsContingencyPlan(MCP)V.GasChromatography(GC)MethodsA.QualityControlRequirementsandPerformanceStandardsforWSC-CAM-VA(PolychlorinatedBiphenylsbyGC)TableofContentsAcronymList31.0QualityControlRequirementsandPerformanceStandardsforWSC-CAM-VA41.1OverviewofWSC-CAM-VA41.2SummaryofSW-846Method8082A61.3SampleExtraction/CleanupMethodsforWSC-CAM-VA71.4MethodInterferences71.5QualityControlRequirementsforWSC-CAM-VA91.6SpecialAnalyticalConsiderationsforWSC-CAM-VA91.7AnalyteListforWSC-CAM-VA232.0DataUsabilityAssessment263.0ReportingRequirementsforWSC-CAM-VA263.1GeneralReportingRequirementsforWSC-CAM-VA263.2SpecificReportingRequirementsforWSC-CAM-VA26ListofTablesandAppendicesTableVA-1SpecificQCRequirementsandPerformanceStandardsforWSC-CAM-VA12-22TableVA-2AnalyteListforWSC-CAM-VA25TableVA-3RoutineReportingRequirementsforWSC-CAM-VA27AppendixVA-1SampleCollection,PreservationandHandlingProceduresforPolychlorinatedBiphenylAnalyses28-29AppendixVA-2DataDeliverableRequirementsforDataAudits30-32ACRONYMLISTCAMCompendiumofAnalyticalMethodsMSMatrixspikeCASNChemicalA