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论文题目:环氧大豆油合成新工艺论文题目:专业:化学工程与工艺(签名)签名)(签名)签名)本科生:指导老师:指导老师:摘要环氧大豆油是国内外开发应用较早的一种环氧型增塑剂,由于具有良好的耐热性、耐光性、互渗性、低温柔韧性,且挥发度低,没有毒性,所以应用相当广泛,特别是用于食品和药物塑料包装材料的增塑剂。甲酸使用量过多容易对设备造成腐蚀,对设备要求高,生产成本大,并且对环境污染严重,本研究采用浸渍法制备出以滑石粉负载三氧化钼的催化剂,为了减少甲酸的用量或者不使用甲酸,以达到清洁生产的目的。在研究中着重讨论了反应时间、甲酸、双氧水、催化剂用量对反应的影响,取得了最佳实验结果所需的原料配比为:大豆油:双氧水:催化剂:甲酸=10g:20g:0.06g:1.4g,反应温度为65℃,反应时间为8h。关键词:关键词:环氧大豆油,双氧水,反应时间,催化剂,甲酸Subject:Epoxysoybeanoilsynthesistechniques:Name:LiangNiInstructor:HeYongJun:(Signature)(Signature)Specialty:ChemistryEngineeringandTechnologyAbstractEpoxysoybeanoilisanepoxytypeplasticizerwhichhasbeenapplicationdevelopmentearlierindomesticandforeign,becauseofitsgoodheatresistance,resistancetolight,mutualpermeability,lowtemperatureflexibility,lowintensity,lowvolatile,andnotoxicity,soitisquitewidespread,especiallyusedforfoodanddrugsplasticizerofplasticpackagingmaterials.Usingtoomuchformicacidwillcorrodeequipmenteasily,equipmentdemandandtheproductioncostishigh,italsopollutetheenvironmentseriously.Inthestudy,usedthecatalystbytheimpregnationmethodofusingtalcumpowderfortheloadofmolybdenumtrioxide,inordertoreducetheamountofacidornotuseformicacid,inordertoachievethepurposeofcleanerproduction.Inthestudyfocusesonthereactiontime,theinfluenceofthecontentofformicacid,hydrogenperoxide,catalysttothereaction,madethebestresultsoftheratioofrawmaterialsneededfor:Soybeanoil:H2O2:Catalyst:Formicacid=10g:20g:0.06g:1.4g,reactiontemperatureat65℃,reactiontimeis8h.KeyWords:Epoxysoybeanoil,Hydrogenperoxide,Reactiontime,Catalyst,Formicacid目录第一章绪论...............................................................................................................................11.1研究背景...............................................................................................................11.2环氧大豆油的性能与用途..................................................................................21.2.1环氧大豆油的性能...................................................................................21.2.1氧大豆油的用途...............